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引用本文:   范咏梅, 张纪梅, 米超, 蔡宇玲, 张丽萍, 朱海彬. 聚二烯丙基二甲基氯化铵改性石墨烯/氧化锌复合材料的制备及在尿酸检测中的应用. 分析化学, 2018, 46(1): 33-38. doi:  10.11895/j.issn.0253-3820.171059 [复制]

Citation:   FAN Yong-Mei, ZHANG Ji-Mei, MI Chao, CAI Yu-Ling, ZHANG Li-Ping, ZHU Hai-Bin. Preparation of Polydiallyl Dimethyl Ammonium Chloride Modified Reduced Graphene Oxide/Zinc Oxide Composite Materials and Its Application in Detection of Uric Acid. Chinese Journal of Analytical Chemistry, 2018, 46(1): 33-38. doi: 10.11895/j.issn.0253-3820.171059 [复制]

聚二烯丙基二甲基氯化铵改性石墨烯/氧化锌复合材料的制备及在尿酸检测中的应用

通讯作者:  张纪梅, zhangjimei6d311@163.com

收稿日期: 2017-07-03

接受日期: 2017-09-29

出版日期: 2018-01-20

基金项目: 本文系国家自然科学基金项目(No.21106101)资助

Preparation of Polydiallyl Dimethyl Ammonium Chloride Modified Reduced Graphene Oxide/Zinc Oxide Composite Materials and Its Application in Detection of Uric Acid

Corresponding author:  ZHANG Ji-Mei, zhangjimei6d311@163.com

Received Date:  2017-07-03

Accepted Date:  2017-09-29

Published Date:  2018-01-20

Fund Project:  This work was supported by the National Natural Science Foundation of China (No. 21106101)

以水合肼为还原剂,硝酸锌为前驱体,采用原位还原法同时还原氧化石墨烯(GO)和硝酸锌,制备了聚二烯丙基二甲基氯化铵(PDDA)改性石墨烯/氧化锌复合材料(PDDA-rGO/ZnO)。采用傅里叶红外光谱(FTIR)、X射线衍射(XRD)和透射电子显微镜(TEM)对复合材料进行了表征,并通过循环伏安(CV)和线性扫描伏安(LSV)电化学测试方法,研究了PDDA-rGO/ZnO修饰玻碳电极对尿酸(UA)的检测性能。结果表明,此修饰电极对UA表现出良好的电催化活性,具有良好的抗干扰性、重现性和稳定性。采用线性扫描伏安法检测UA的线性范围为0.02~0.10 mmol/L和0.10~1.00 mmol/L,检出限为15.9 nmol/L(S/N=3)。

关键词:   石墨烯, 氧化锌, 复合材料, 循环伏安, 线性扫描, 尿酸
Key words:   Graphene, Zinc oxide, Composite material, Cyclic voltammetry, Linear sweep voltammetry, Uric acid
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目录

聚二烯丙基二甲基氯化铵改性石墨烯/氧化锌复合材料的制备及在尿酸检测中的应用

范咏梅, 张纪梅, 米超, 蔡宇玲, 张丽萍, 朱海彬

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