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引用本文:   王林玉, 洪莎莎, 黎艳艳, 宋永海, 汪莉. 三维多孔碳/共价有机框架材料自支撑电极用于多巴胺电化学传感分析. 分析化学, 2021, 49(6): 1053-1060. doi:  10.19756/j.issn.0253-3820.210418 [复制]

Citation:   WANG Lin-Yu , HONG Sha-Sha , LI Yan-Yan , SONG Yong-Hai , WANG Li . Dopamine Electrochemical Sensor Based on Three-Dimensional Macroporous Carbon/Covalent Organic Framework Integrated Electrode. Chinese Journal of Analytical Chemistry, 2021, 49(6): 1053-1060. doi: 10.19756/j.issn.0253-3820.210418 [复制]

三维多孔碳/共价有机框架材料自支撑电极用于多巴胺电化学传感分析

通讯作者:  汪莉, lwang@jxnu.edu.cn

收稿日期: 2021-04-07

基金项目: 国家自然科学基金项目(Nos.21765009,21964010,21465014,21665012)资助。

Dopamine Electrochemical Sensor Based on Three-Dimensional Macroporous Carbon/Covalent Organic Framework Integrated Electrode

Corresponding author:  WANG Li , lwang@jxnu.edu.cn

Received Date:  2021-04-07

Fund Project:  Supported by the National Natural Science Foundation of China (Nos.21765009, 21964010, 21465014, 21665012).

通过简单的水热法使二苯甲酸二肼和1,3,5-三(对甲酰基苯基)苯发生氨醛缩合反应,合成了一种新的共价有机框架材料(COFTFPB-TDF)。将COFTFPB-TDF生长到三维多孔碳(3D-KSC)上,得到3D-KSC/COFTFPB-TDF自支撑电极,采用扫描电子显微镜进行结构表征,结果表明,3D-KSC/COFTFPB-TDF具有片层结构,同时含有很多孔洞,可以固载其它的材料。采用循环伏安法研究了3D-KSC/COFTFPB-TDF自支撑电极对多巴胺的检测性能。结果表明,此传感器对多巴胺表现出良好的传感性能,具有低的检出限(0.045 μmol/L)、宽的线性范围(0.13 μmol/L~0.06 mmol/L)和高灵敏度(369 μA/(mmol/L)/cm2),这主要归因于COFTFPB-TDF较大的比表面积和较多的孔洞结构。因此,此材料具有良好的应用前景。

关键词:   共价有机框架材料, 多巴胺, 电化学传感器, 三维多孔碳
Key words:   Covalent organic framework, Dopamine, Electrochemical sensor, Three-dimensional macroporous carbon
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目录

三维多孔碳/共价有机框架材料自支撑电极用于多巴胺电化学传感分析

王林玉, 洪莎莎, 黎艳艳, 宋永海, 汪莉

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